Effect of sonication time on the synthesis of the CdS nanoparticle based multiwall carbon nanotube - maleic anhydride-1-octene nanocomposites
FULLERENES NANOTUBES AND CARBON NANOSTRUCTURES, cilt.26, sa.5, ss.255-262, 2018 (SCI-Expanded, Scopus)
- Yayın Türü: Makale / Tam Makale
- Cilt numarası: 26 Sayı: 5
- Basım Tarihi: 2018
- Doi Numarası: 10.1080/1536383x.2018.1432602
- Dergi Adı: FULLERENES NANOTUBES AND CARBON NANOSTRUCTURES
- Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
- Sayfa Sayıları: ss.255-262
- Açık Arşiv Koleksiyonu: AVESİS Açık Erişim Koleksiyonu
- İstanbul Üniversitesi-Cerrahpaşa Adresli: Hayır
Özet
Effect of sonication time on the synthesis of the CdS nanoparticles within the matrix obtained through the covalent functionalization of multiwall carbon nanotube (MWCNT) with maleic anhydride (MA) - 1-octene copolymer was investigated. Cadmium chloride and thiourea were used as the raw materials. MWCNTs used for the matrix were synthesized by Catalytic Chemical Vapor Deposition using Fe-Co/Al2O3 as the catalyst. The obtained nanostructures were characterized by FTIR, XRD, Raman spectroscopy, TEM, SEM, TG and UV-Vis spectroscopy. Electrophysical properties of the polymer nanocomposites obtained using different periods of time for sonication were comparably investigated. The average CdS particle diameter was between 3.9-7.9nm as confirmed independently by TEM and XRD. UV-Vis spectroscopy revealed that the obtained nanostructures are appropriate base materials for making optical devices.