International Academic Studies Conference, Ankara, Turkey, 3 - 05 August 2022, pp.1, (Summary Text)
The preparation and characterization of CMC- silica composites: Digital
characterization
Elif Tüzün
Istanbul University-Cerrahpasa, Department of Chemistry, Istanbul (34320), Turkey.
elif.tuzun@istanbul.edu.tr
Abstract
The fabrication of green and low-cost biopolymer-based nanocomposites (NCs) has been
given great attention because of their unique physicochemical characteristics such as particle
size, shape, and distribution of structures in nanotechnological applications. In recent years,
biopolymer-based NCs have been reported to exhibit excellent biological, chemical, physical,
and mechanical properties. Herein, we prepared novel carboxymethyl cellulose (CMC)-
Silica NCs using a green and low–cost sonication method at room temperature. The prepared
CMC- Silica NCs were characterized using different advanced techniques such as High
Resolution Transmission Electron Microscopy (HRTEM) and Fourier Transform Infrared
(FTIR) spectroscopy. In this study, we investigated the surface property of the green CMC-
Silica NCs using an artificial intelligence. (AI) approach. The HRTEM micrograph of the
green CMC- Silica NCs was analyzed using a simple and easy-to-
use Image software. According to the surface experimental results, we observed that the sono-
prepared CMC- Silica NCshad a spherical shape with a uniform distribution ranging from 34
nm to 66 nm. In Fig. 1, the HRTEM micrograph and AI supported HRTEM micrograph of the
green CMC- Silica NCs were presented (8 bit and Rainbow RGB mode). Consequently, we
concluded that the prepared CMC-Silica NCs are a promising nanomaterial in biomedical
applications with a uniform particle size distribution under the optimum experimental
conditions.
Figure 1: (a) The HRTEM micrograph of and (b) AI supported HRTEM micrograph of the
green CMC- Silica NCs.
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